synthesis of 1,2-disubstituted benzimidazoles in the presence of sba-pr-so3h as a nano solid acid catalyst
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abstract
in this article, simple, convenient synthesis of 2-aryl-1-arylmethyl-1h-1,3-benzimidazole (1,2-disubstitutedbenzimidazoles) via condensation of 1,2-phenylenediamine and aromatic aldehydes using sba-pr-so3h as a nanoporous solid acid catalyst in green protocol was reported.
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Sulfonic acid functionalized nanoporous silica (SBA-Pr-SO3H) with a pore size of 6 nm catalyzed three component coupling of aromatic aldehydes, urea and ethyl acetoacetate to afford the corresponding dihydropyrimidinones under solvent free condition. This new protocol for Biginelli reaction has important advantages such as green synthesis, short reaction time, easy isolation and high yields of ...
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Journal title:
journal of nanostructuresPublisher: university of kashan
ISSN 2251-7871
volume 2
issue 2 2012
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